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Single-crystal 3D electron diffraction dataset for ammonium oxalate monohydrate

Version 1.0

Kulik, Marta; Olech, Barbara; Dominiak, Paulina, 2025, "Single-crystal 3D electron diffraction dataset for ammonium oxalate monohydrate", https://doi.org/10.18150/EAK27N, RepOD, V1

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Description

Electron diffraction dataset collected from ammonium oxalate monohydrate (Sigma-Aldrich) micro crystals, as supplied by the manufacturer.

Microscope: Thermo Fisher Scientific 200kV Glacios Transmission Electron Microscope (Cryomicroscopy and Electron Diffraction Core Facility at the Centre of New Technologies, University of Warsaw, Poland)

Camera: Ceta-D camera (bin 2x2, rolling shutter, noise reduction mode)

Collection Software: EPU-D (Thermo Fisher), SMV format

Collection Parameters: 200keV, -193C, 50um C2, gun lens 8, spot size 11, extraction voltage 3850V, parallel beam, beam diameter ~1.7 um, beam stop inserted, oscillation per frame 0.4 deg, 0.5 s exposure time, tilt speed 0.8 deg/s, rotation -60 to +60 deg

Grid: lacey carbon Cu 200 mesh glow discharged for 60s at 25mA

Sample: ammonium oxalate monohydrate

(2025-06-15)
Subject
Chemistry
Keyword

electron crystallography, 3D ED, microED, quantum crystallography

CC0 Creative Commons Zero 1.0 CC0 Creative Commons Zero 1.0

1 File
AmmoniumOxalateMonohydrate20230404.zip
ZIP Archive - 1.2 GB - Jul 1, 2025 - 0 Downloads
MD5: 177e837f614a0199970351c709449df9
License: CC0 Creative Commons Zero 1.0
3D electron diffraction images and associated files
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