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Gryko, Dorota; Wincenciuk Aleksandra; Cmoch Piotr; Giedyk Maciej; Andersson Martin P, 2024, "Aqueous Micellar Environment Impacts the Co-Catalyzed Phototransformation: A Case Study", https://doi.org/10.18150/SGJHBJ, RepOD, V1
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In recent years, methodologies that rely on water as the reaction medium have gained considerable attention. The unique properties of micellar solutions were shown to improve the regio-, stereo-, and chemoselectivity of different transformations. Herein, we demonstrate that the aqueous environment is a suitable medium for a visible light driven cobalt-catalyzed reaction involving radical species. In this system, reduced vitamin B12reacts with alkyl halides, generating radicals that are trapped by the lipophilic olefin present in the Stern layer. A series of NMR measurements and theoretical studies revealed the location of reaction components in the micellar system.
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