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Publication raw data: Continuous-flow microreactor for Knoevenagel condensation of ethyl cyanoacetate with benzaldehyde. The effect of grafted amino groups on catalytic activity

Version 1.0

Ciemięga, Agnieszka, 2024, "Publication raw data: Continuous-flow microreactor for Knoevenagel condensation of ethyl cyanoacetate with benzaldehyde. The effect of grafted amino groups on catalytic activity", https://doi.org/10.18150/GFTWT2, RepOD, V1

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Description

Data for Publication: ChemPlusChem

sample designation in the publication: M; M-N1; M-N2; M-N3; M-N4; M-N5


File:ASAP

File format: *xlsx;*csv

Figure 1, Table 1 in manuscript

Data from nitrogen adsorption/desorption measurments.

ASAP2020 Micromeritics; ASAP2020 softwere

Samples degassed at 200 ◦C under vacuum for 24 h. Nitrogen adsorption at −196◦C. The specific surface area calculated using Braunauer, Emmet and Teller (BET) equation; micropore size using the Dubinin–Astakhov equation.


File:FTIR

File format: *csv

Figure 3 in manuscript

Data from FTIR measurments

NICOLET 6700 spectrometer; Thermo Fisher Scientific; OMNIC softwere; DRIFT (5% of sample in KBr); 

Spectra range 400–4000 cm−1; resolution 4 cm−1.


File:TG

File format: *csv

Figure 4, Table 2 in manuscript

Data from thermogravimetric measurments

Star 850, Mettler Toledo. Temperature range of 25-800 °C, heating ramp of 10 deg/min, air rate 60 ml/min


File:Catalytic Experiments

File format:*pdf

Figure 5-10, Table 4 in manuscript

Reports from GC chromatography

Agilent 7890A, flame ionization detector FID; capillary column HP5; Inlet temperature: 250◦C ; sample volume: 1um, split ratio: 5:1; oven temp: 40◦C-200o◦C He flow 6.5 ml/min; detector: temperature 300◦C; H2 flow:30 ml/min, Air flow:400ml/min


Subject
Engineering
Keyword

heterogeneous catalysis, microreactors, monoliths, Knoevenagel condensation, Lewis bases

Related Publication

Continuous-Flow Microreactor for Knoevenagel Condensation of Ethyl Cyanoacetate with Benzaldehyde: The Effect of Grafted Amino Groups on Catalytic Activity; Katarzyna Maresz, Agnieszka Ciemięga, Julita Mrowiec-Białoń,
ChemPlusChem 2023,88,e202200390 https://doi.org/10.1002/cplu.202200390 doi: 10.1002/cplu.202200390

CC0 Creative Commons Zero 1.0 CC0 Creative Commons Zero 1.0

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ASAP.zip
ZIP Archive - 327.0 KB - Feb 22, 2024 - 7 Downloads
MD5: e0a1aa9f14f84b906b5ca3a7b8b06cc5
License: CC0 Creative Commons Zero 1.0
File format: *xlsx;*csv Figure 1, Table 1 in manuscript Data from nitrogen adsorption/desorption measurments. ASAP2020 Micromeritics; ASAP2020 softwere Samples degassed at 200 ◦C under vacuum for 24 h. Nitrogen adsorption at −196◦C. The specific surface area calculated using Braunauer, Emmet and Teller (BET) equation; micropore size using the Dubinin–Astakhov equation.
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FTIR.zip
ZIP Archive - 285.9 KB - Feb 22, 2024 - 1 Download
MD5: 728890a34dbc4bd4e0dfc924bdc8ab4b
License: CC0 Creative Commons Zero 1.0
File format: *csv Figure 3 in manuscript Data from FTIR measurments NICOLET 6700 spectrometer; Thermo Fisher Scientific; OMNIC softwere; DRIFT (5% of sample in KBr); Spectra range 400–4000 cm−1; resolution 4 cm−1.
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GC.zip
ZIP Archive - 6.7 MB - Feb 22, 2024 - 3 Downloads
MD5: fd2cae43a8c186a9f442955567821cdf
License: CC0 Creative Commons Zero 1.0
File format:*pdf Figure 5-10, Table 4 in manuscript Reports from GC chromatography Agilent 7890A, flame ionization detector FID; capillary column HP5; Inlet temperature: 250◦C ; sample volume: 1um, split ratio: 5:1; oven temp: 40◦C-200o◦C He flow 6.5 ml/min; detector: temperature 300◦C; H2 flow:30 ml/min, Air flow:400ml/min
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TG.zip
ZIP Archive - 16.9 KB - Feb 22, 2024 - 1 Download
MD5: f1cae5a6ffac8b6f9f9c5905e3dfa1d6
License: CC0 Creative Commons Zero 1.0
File format: *csv Figure 4, Table 2 in manuscript Data from thermogravimetric measurments Star 850, Mettler Toledo. Temperature range of 25-800 °C, heating ramp of 10 deg/min, air rate 60 ml/min
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