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Dębski, Adam, 2026, "Experimental and Theoretical Investigation of the κ-Phase (Ag2Mg5) in the Ag-Mg System", https://doi.org/10.18150/64UOD7, RepOD, V1
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There is a limited number of works on the κ-phase from the Ag-Mg system in the currently available literature. The thermodynamic properties of the phase are mostly based on calculations. In view of the above, the present study is a continuation of research on the thermodynamic properties of the Ag-Mg system. The main objective of this work is to expand current knowledge, with a special focus on the κ-Ag2Mg5 phase. The scope of work has been divided into two parts. The experimental part of the study includes the synthesis of the κ-phase from high-purity Ag and Mg, as well as results from scanning electron microscopy (SEM) and X-ray diffraction (XRD). Prepared material was then utilised for calorimetric measurements of the standard enthalpy of formation with the use of the drop solution calorimetry method. In the theoretical part of the study, defect formation energy was determined using the ab initio calculations
Provided data set contains the raw data from the experimental part of the article:
1. .txt files with column headers Index Time (h) Furnace Temperature (°C) Sample Temperature (°C) Heat Flow (µV) contain calorimetric data of the formation enthalpy measurements for the Ag2Mg5 alloy in a tin and aluminum bath.
2. .xy files are XRD diffraction patterns for the alloy used for the enthalpy of formation measurements.
3. .TIFF files are SEM images of alloys used for the enthalpy of formation measurements.
This work is supported by the National Science Centre, Poland, for funding project no. 2021/43/O/ST8/01291 entitled “Thermodynamic properties and structure of Cu-Mg-Ti and Ag-Mg-Ti alloys and their potential to interact with hydrogen” in the years 2022–2027.
κ-Ag2Mg5 phase, enthalpy of formation, thermodynamic properties, calorimetry, ab initio calculation, defect formation energy
W. Gozdur, W. Gierlotka, M. Bieda, W. Gąsior, A. Budziak, M. Polański, M. Pęska, A.Dębski, Experimental and Theoretical Investigation of the κ-Phase (Ag2Mg5) in the Ag-Mg System, Materials, 19(11), (2026), 2241. https://doi.org/10.3390/ma19112241 doi: 10.3390/ma19112241
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