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Raw data for project „Synthesis of new water-insoluble β-ketoimines, obtained from β-diketone derivatives and aminosilanes, capable of binding metal ions from aqueous solutions”, folder 2

Version 1.0

Witt, Katarzyna, 2024, "Raw data for project „Synthesis of new water-insoluble β-ketoimines, obtained from β-diketone derivatives and aminosilanes, capable of binding metal ions from aqueous solutions”, folder 2", https://doi.org/10.18150/01AFBV, RepOD, V1

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Description

The data was obtained as a part of a project entitled "Synthesis of new water-insoluble β-ketoimines obtained from derivatives of β-diketones and aminosilanes, capable of binding metal ions from aqueous solutions" no. 2023/07/X/ST4/00361 (Miniatura 7) financed by the National Science Center (Poland) (NCN). The file contains raw data and metadata related to the structural characteristics of the obtained β-ketoimines and data related to determined stability constants of β-ketoimine complexes with selected metal ions:

  • Bruker Advance 3HD 400 MHz spectrometer – spectra of 1H, 13C NMR recorded in a DMSO-d6, 99.8% atom %D solution
  • Bruker Alpha-PFT-IR device with a diamond attenuated total reflectance (ATR) accessory - FTIR-ATR spectra of obtained β-diketones
  • UV-Vis spectrophotometry Varian Cary 50 – absorption spectra of complexes obtained in various molar ratios of β-ketoimines and metal ions (Ag+, Au3+, Cd2+, Co2+, Cr6+, Cu2+, Fe3+, Mg2+, Ni2+, Pd2+, Pt2+, and Zn2+) recorded in methanol-aqueous solutions in the range from 200 to 550 nm, with spectral slits at 0.5 nm and 0.2 nm steps using curettes with path lengths of 1 cm


(2024-07-18)
Subject
Chemistry; Earth and Environmental Sciences
Keyword

synthesis, β-ketoimines, β-diketones, aminosilanes, complex compounds

2026-07-31

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